Chemical Laboratory Instrumentation: Operation, Quality and Safety of Equipment
Details :
Efficient use of advanced operations and instruments in the
chemical laboratory are vital tools to solve any laboratory problem. The course
provides basic laboratory analysis methods and troubleshooting techniques for
the most used instruments. Laboratory quality management according to an
international standard is also important to enhance the laboratory system and
environment. In addition, safety regulations are increasingly emphasizing the
importance of management commitment and employee involvement in managing risks.
The aim of this course is to enrich and advance the skills and knowledge of
participants to understand laboratory techniques, quality laboratory
requirements and the procedures of safety methods.
This course will links together an understanding of performance
characteristics with an appreciation of the limitations imposed by analytical
instrument design, leading to the interplay of the validation and qualification
processes within quality assurance systems. The course includes unique
framework of topics covers the major instrumental techniques of
spectrophotometry, chromatography, capillary electrophoresis and atomic
emission spectroscopy. The use of case studies, exercises and practical
applications, will help the participants to develop a thorough understanding of
the various concepts that underpin the different techniques.
This course will cover the major operations performed in an
industrial chemical laboratory. It will describe the major equipment used in
the chemical laboratory, their operations, validations, calibrations and
maintenance. The course will concentrate on Standard Operation Procedures (SOP)
which includes development, revisions, standards and implementations. Various
Quality standards will be discussed. However, the course will concentrate on
ISO 17025:2005. Finally, the course will demonstrate the safety practices and
its critical impact in an industrial chemical laboratory. OSHA standards and
regulations will be discussed and related videos will be shown to attendees.
In addition to the updated
knowledge provided to attendees during the course period, each attendee will go
back to his/her laboratory equipped with an outstanding manual that includes typical
SOP’s that can be modified and used within attendee’s laboratory.
This outstanding course is a MUST for every laboratory
professional. The updated knowledge and techniques covered during the 5 days of
this training, will dramatically improve not only the attendee’s skills, but
will also improve the performance of the attendee’s laboratory as a whole. However,
if you are looking to improve the performance of your laboratory, then you have
to commit yourself to pass the knowledge gained in this training to your
subordinates and colleagues back in your laboratory as we will give you all the
tools needed for this purpose; knowledge, skills, manual, power point slides,
videos, Standard Operation Procedures (SOP), forms and standards.
Ø Upon successful completion of this course, the delegates will be able to:
Apply an in-depth knowledge and
skills in the chemical laboratories including analytical instrumentation,
analytical techniques, laboratory equipment, operational procedures, management
style, method validation, quality and safety management systems
Use the major analytical
laboratory instruments and equipment and understanding their performance
characteristics, capabilities, accuracies, reliabilities, speed and limitations
including UV/VIS, flow injection, infrared/raman spectroscopy, ion
chromatography, pH probes, and gas chromatography
Calibrate and certify various
laboratory instruments and calculate uncertainty and random error
Impart the participants
fundamental techniques of chemical laboratory
Understand how to validate the
analytical method
Analyse the instrument
performance characteristics which includes types and interaction between
different characteristics
Prepare and handle sample for
different analytical instrumentations and extract analyses from complex
matrices
Develop and modify the laboratory
standard operation procedures (SOP) and interpret the requirements of the ISO
17025 quality system
Explain the flow of work and
major concerns related to the Industrial Chemical Laboratory
Carryout sampling and sample
handling
Increase knowledge about laboratory equipment and instruments such as mechanical measurements, chemical analysis and process analysers
Discuss nuclear magnetic
instruments covering its theory, NMR spectroscopy, design and performance idea
Illustrate NMR applications,
multi-dimensional NMR spectroscopy and solid-state NMR spectroscopy
Perform chemical laboratory
operations and gain good skills of developing and modifying the laboratory
Standard Operating Procedures (SOP)
To understand the laboratory
quality requirements and appreciate the need for a quality system according to
the International Standards Organization ISO 17025 standard
To use the international Guide to
Lab Quality for accreditation standard methods
Employ the safety and
environmental requirements for chemical laboratory as per OSHA standard
This
course provides an overview of all significant aspects and considerations of
modern chemical laboratory for those who are involved in analytical
instrumentation, equipment calibration, operations, quality and safety
including laboratory managers, engineers, chemists, scientists and other
laboratory technical staff. This course is also suitable for instrumentation
engineers and other instrumentation staff who are in-charge of instrumentation
calibration and maintenance
Day 1:
ü
Introduction to chemical
laboratory technique
ü
Preparation of chemicals
Day 2:
ü
High performance liquid
chromatography: mobile phase, pumping system, sample inject system, column,
detector types
ü
Data management software
ümulti-dimensional NMR spectroscopy
Day 3:
ü
Quantitative methods: calibration
methods, external and internal standards, outliers test, determination of
analytes concentration, standard addition method, error in quantitative
analysis, confidence limits, detection limit, repeatability and reproducibility
Day 4:
ü üTransporting of chemicals
ü üElectrical safety
ü ü Practical Session/Site Visit
ü
Day 5:
ü
Guidelines for good laboratory
practices
- All lectures are in colorful presentation
- All lectures are interspersed with interactive discussion
- All lectures include group discussion, case history and exercises
- Actual major incidents as well as industry experience are reviewed
- Participants receive a multicolor course manual
- Pictures of real incidents and case history are shown
- Videos on the subject are shown
daily 09:00 – 14:00